№ files_lp_4_process_3_081583
Checklist for laboratory procedures and quality control compliance for ammonia nitrogen analysis using approved and modified EPA methods, including sample preservation, equipment, reagents, and documentation requirements.
Year: 1993
Region / City: North Carolina, USA
Subject: Water quality analysis, ammonia nitrogen measurement
Document Type: Laboratory checklist / Standard Operating Procedure verification
Agency: North Carolina Department of Environmental Quality / Division of Water Resources
Primary Analyst: [Not specified]
Prepared by: [Name of person completing checklist]
Equipment: Spectrophotometer, pH meter, borosilicate glass distillation equipment
Methods: EPA Method 350.1 Rev. 2.0, Hach Method 10205 TNT
Reagents: Borate buffer, boric acid solution, ammonia-free water, Hach TNTplus kits, NaOH, dechlorinating reagent, sulfuric acid, sodium hypochlorite, sodium phenolate, sodium nitroprusside, EDTA buffer
QC Requirements: Compliance with EPA 350.1 Rev. 2.0 for modified methods
Sample Handling: Preservation with H2SO4 to pH <2, refrigerated transport ≤6 ºC, analysis within 28 days
Regulatory References: 40 CFR Part 136, 15A NCAC 2H .0805, SM 4500 NH3 B-2011
Price: 8 / 10 USD
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