№ files_lp_3_process_9_62101
Laboratory instructional guide outlining the dehydration of cyclohexanol with concentrated phosphoric acid, subsequent distillation and purification of cyclohexene, associated safety precautions, required apparatus and reagents, and yield determination within an organic chemistry practical framework.
Title: Preparation of Cyclohexene
Unit: Unit 3 PPA 1
Subject Area: Chemical Investigations
Topic: Organic Chemistry
Experiment Focus: Dehydration of cyclohexanol to form cyclohexene
Type of Document: Laboratory experiment guide
Intended Audience: Teachers and laboratory technicians
Chemicals Involved: Cyclohexanol, 85% phosphoric acid, cyclohexene, sodium chloride solution, anhydrous calcium chloride, bromine solution
Apparatus: Distillation setup with round-bottomed flasks, condenser, separating funnel, heating mantle, thermometer
Safety Requirements: Use of eye protection and gloves; handling of corrosive, flammable and toxic substances
Procedure Elements: Distillation, liquid-liquid separation, drying of organic layer, purification, yield calculation, unsaturation test
Assessment Component: Calculation of percentage yield and confirmation of unsaturation
Price: 8 / 10 USD
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