№ lp_1_2_49266
Checklist addressing laboratory practices, sample handling, calibration, and quality control requirements for nitrite nitrogen analysis under North Carolina certification and EPA Method 353.2.
Organization: North Carolina Department of Environmental Quality, Division of Water Resources
Branch: Wastewater/Groundwater Laboratory Certification Branch
Document type: Laboratory quality assurance and compliance checklist
Analytical parameter: Nitrogen, Nitrite
Analytical method: EPA Method 353.2, Revision 2.0 (1993)
Analytical technique: Automated continuous-flow analysis with cadmium reduction bypassed
Applicable regulations: 15A NCAC 2H .0805; 40 CFR 136
Equipment: Automated continuous-flow analyzer; analytical balance
Reagents: Color reagent; reagent water; wash solution; dilute hydrochloric acid; ammonium chloride-EDTA solution; nitrate and nitrite stock and standard solutions
Sample preservation and storage requirements: Refrigeration ≤ 6 °C; analysis within 48 hours
Calibration requirements: Multi-point calibration with blank; correlation coefficient ≥ 0.995
Quality control: Second-source Quality Control Standard; ongoing calibration verification
Intended use: Laboratory compliance review and certification assessment
Price: 8 / 10 USD
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